Formic acid: A low-cost, mild, ecofriendly, and highly efficient catalyst for the rapid synthesis of β-enaminones

Siddappa A. Patil; Phillip A. Medina; Diego Gonzalez-Flores; Jason K. Vohs; Seth Dever; Leslie W. Pineda; Mavis L. Montero; Bradley D. Fahlman

doi:10.1080/00397911.2012.708467

Formic acid: A low-cost, mild, ecofriendly, and highly efficient catalyst for the rapid synthesis of β-enaminones

Siddappa A. Patil, Phillip A. Medina, Diego Gonzalez-Flores, Jason K. Vohs, Seth Dever, Leslie W. Pineda, Mavis L. Montero, Bradley D. Fahlman

Research output: Contribution to journal › Article › peer-review

10 Scopus citations

Abstract

β-Enaminones have been synthesized by the condensation reaction of b-diketones with various anilines in the presence of a catalytic amount of formic acid, mild and highly efficient acid catalyst in methanol. These condensation reactions proceed smoothly in short reaction times with near-quantitative yields.

Original language	English
Pages (from-to)	2349-2364
Number of pages	16
Journal	Synthetic Communications
Volume	43
Issue number	17
DOIs	https://doi.org/10.1080/00397911.2012.708467
State	Published - Sep 2 2013

Keywords

Crystal structure
Formic acid
Synthesis
β-enaminone

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abstract = "β-Enaminones have been synthesized by the condensation reaction of b-diketones with various anilines in the presence of a catalytic amount of formic acid, mild and highly efficient acid catalyst in methanol. These condensation reactions proceed smoothly in short reaction times with near-quantitative yields.",

keywords = "Crystal structure, Formic acid, Synthesis, β-enaminone",

author = "Patil, {Siddappa A.} and Medina, {Phillip A.} and Diego Gonzalez-Flores and Vohs, {Jason K.} and Seth Dever and Pineda, {Leslie W.} and Montero, {Mavis L.} and Fahlman, {Bradley D.}",

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AU - Patil, Siddappa A.

AU - Medina, Phillip A.

AU - Gonzalez-Flores, Diego

AU - Vohs, Jason K.

AU - Dever, Seth

AU - Pineda, Leslie W.

AU - Montero, Mavis L.

AU - Fahlman, Bradley D.

PY - 2013/9/2

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AB - β-Enaminones have been synthesized by the condensation reaction of b-diketones with various anilines in the presence of a catalytic amount of formic acid, mild and highly efficient acid catalyst in methanol. These condensation reactions proceed smoothly in short reaction times with near-quantitative yields.

KW - Crystal structure

KW - Formic acid

KW - Synthesis

KW - β-enaminone

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DO - 10.1080/00397911.2012.708467

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JO - Synthetic Communications

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ER -

Formic acid: A low-cost, mild, ecofriendly, and highly efficient catalyst for the rapid synthesis of β-enaminones

Abstract

Keywords

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